Application of high-performance liquid chromatography / high resolution mass spectrometry for investigation of sodium 2,3-disulfanyl- 1-propanesulfonate (unithiol) and products of its oxidation with hydrogen peroxide
T13N2
D.O. Kuleshov, T.E. Berezkina, Y. V. Russkikh, E. N. Chernova, Z. A. Zhakovskaya,
S.V. Masyukevich, L.N. Gall, N.R. Gall
High-performance liquid chromatography combined with high resolution mass spectrometry has been used to study soft oxidation of sodium 2,3-disulfanyl-1-propanesulfonate (unithiol) with hydrogen peroxide; reference peaks were identified for initial substance and reaction products. The possibility to use high-performance liquid chromatography with high resolution mass spectrometry for Sokolovsky thiol-disulphide test has been shown.
